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瀛﹁€呴檲澶ч挦 鍙戣〃浜?010-1-8 11:50:56
锛? 鈹? 娴忚锛?97      

闈㈠悜涓孩澶栧簲鐢ㄧ殑纭崵鐜荤拑闄剁摲鍏夊姛鑳芥潗鏂?/span>

3-10um娉㈡鐨勪腑绾㈠婵€鍏夊湪OPO锛堝厜鍙傞噺鎸崱鍣級婵€鍏夊櫒鏄鐩栬繖浜涙尝娈电殑鍏稿瀷婵€鍏夌郴缁燂紝浣嗙敱浜庨渶瑕侀潪绾挎€ф櫠浣撲互鍙婃车娴︽縺鍏夋簮閰嶅悎浣滅敤锛?/span>OPO婵€鍏夊櫒鍏夊绯荤粺鐨勮璁′笌鏋勯€犲崄鍒嗗鏉傘€備竴绉嶇畝鍗曞彲琛岀殑瑙e喅鍔炴硶鏄洿鎺?a name="OLE_LINK19">閲囩敤涓孩澶栧浐鎬佹縺鍏夊櫒浠?/a>锛屽畠瑕佹眰鏈夊悎閫傜殑婵€娲荤瀛愬拰鍩轰綋浠嬭川銆傜█鍦熺瀛愬銆?/span>Er3+銆?/span>Tm3+銆?/span>Dy3+銆?/span>Pr3+绛夎兘绾х粨鏋勫鏉傦紝鍦ㄤ腑绾㈠鍖哄煙鍏锋湁涓板瘜鐨勫彂灏勬尝娈点€備絾瀵逛簬鐩墠琚箍娉涚爺绌剁殑姘у寲鐗╁拰姘熷寲鐗╃幓鐠冩垨鏅朵綋鍩轰綋锛岀敱浜庡叾澹板瓙鑳介噺杈冮珮锛屾幒鏉傜殑绋€鍦熺瀛愬湪涓孩澶栧尯鍩熺殑鏃犺緪灏勮穬杩佸嚑鐜囪緝澶э紝瀵艰嚧鍙戝厜鏁堢巼浣庛€傚洜姝わ紝鐮旂┒鍏锋湁浣庡0瀛愯兘閲忋€佷笖鐗╁寲鎬ц兘绋冲畾鐨勫熀浣撴潗鏂欐垚涓哄彂灞曚腑绾㈠鍥轰綋婵€鍏夊櫒鐨勫叧閿幆鑺傘€?/span>

鐩告瘮浜庢哀鍖栫墿鎴栨盁鍖栫墿锛屾隘鍖栫墿鏅朵綋鍏锋湁鏇翠綆鐨勫0瀛愯兘閲忥紝濡傛隘鍖栭暓锛?/span>LaCl3锛夋櫠浣撶殑鏈€澶у0瀛愯兘閲忕害涓?/span>210cm-1锛岃繙浣庝簬姘熷寲闀э紙LaF3锛夌殑澹板瓙鑳介噺锛堢害涓?/span>400cm-1锛夈€傜洰鍓嶅凡鎶ラ亾鐨勭█鍦熺瀛愭渶闀挎尝闀匡紙7.2um锛夌殑婵€鍏夊彂灏勬鏄€氳繃鍦ㄦ隘鍖栭暓鏅朵綋涓幒鍏?/span>Pr3+绂诲瓙瀹炵幇鐨?/span>[1]銆備絾鐢变簬璇ユ潗鏂欐槗鍚告按锛岄渶瑕佺壒娈婄殑澶勭悊鍜屽偍瀛橈紝鍥犺€岄檺鍒朵簡鍏跺疄闄呭簲鐢ㄣ€?/span>

纭崵鐜荤拑鏄~绯诲寲鍚堢墿鍜屽崵鍖栫墿鎴栬€呭畠浠殑鍗曡川鍏冪礌娣峰悎鐔斿埗鎴愮殑鐜荤拑鎬佹潗鏂欍€傚畠鍏锋湁纭郴鐜荤拑楂樼殑鍖栧绋冲畾鎬у拰鍔涘鎬ц兘锛屽悓鏃跺張鍏锋湁鍗ゅ寲鐗╃幓鐠冧綆鏈緛鎹熻€楃殑鐗圭偣;姝ゅ锛屽叾绾㈠閫忚繃鑼冨洿骞匡紙鍙揪鍒拌繙绾㈠锛夈€佷笖閫忚繃鐜囬潪甯搁珮锛屽洜姝よ繎骞存潵浣滀负绾㈠鍏夊绐楀彛鏉愭枡琚箍娉涚爺绌?/span>[2-6]銆傚彟澶栵紝鐢变簬纭崵鐜荤拑鍏锋湁浣庡0瀛愯兘閲忓拰楂樻姌灏勭巼锛屾幒鍏ョ█鍦熸縺娲讳腑蹇冨悗锛屼篃鍙互浣滀负涓繙绾㈠鍙戝厜鏉愭枡[7-12]銆備絾鏄紝鐩稿浜庢櫠浣撹€岃█锛?a name="OLE_LINK39">鐜荤拑鏉愭枡涓█鍦熺殑鍙戝皠璋辩嚎杈冨锛堝瓨鍦ㄩ潪鍧囧寑灞曞锛夛紝瀵艰嚧鍏跺彂灏勬埅闈㈣緝浣庯紝涓嶅埄浜庤幏寰楅珮鏁堟縺鍏夎緭鍑恒€?/span>

閫忔槑绾崇背缁撴瀯鐜荤拑闄剁摲锛堢敱鏃犳満鐜荤拑鍙戠敓閮ㄥ垎鏅跺寲鑰屽緱锛屾槸鐜荤拑鐩镐笌绾崇背鏅剁浉鐨勫鍚堜綋锛夋槸涓€绫诲緢鏈夊墠閫旂殑鏂板瀷鍏夊姛鑳界撼绫冲鍚堟潗鏂欙紝瀹冪患鍚堜簡鏅朵綋涓庣幓鐠冩潗鏂欑殑浼樼偣锛屽彲鍏锋湁涓庢櫠浣撶浉杩戠敋鑷虫洿濂界殑鍏夊鎬ц兘锛岃€屽張鏈夌被浼间簬鐜荤拑鏉愭枡鍒跺鎶€鏈畝鍗曘€佹垚鏈綆鍜屽彲楂樻祿搴︽幒鏉傜殑鏄庢樉浼樺娍锛涙澶栵紝璇ュ鍚堟潗鏂欑殑鍔涘鎬ц兘鍜岀儹绋冲畾鎬э紙涓昏鍙栧喅浜庣幓鐠冪浉鍩轰綋锛変篃涓庝竴鑸棤鏈虹幓鐠冪浉褰撱€傝浣胯绫荤撼绫冲鍚堟潗鏂欏叿鏈変紭寮傜殑鍙戝厜鎬ц兘锛屾幒鏉傜殑绋€鍦熸縺娲荤瀛愬ぇ閮ㄥ垎浠ョ疆鎹㈠浐婧剁殑鏂瑰紡杩涘叆鏋愬嚭鐨勭撼绫虫櫠鐩镐腑鏄潪甯搁噸瑕佺殑[13]銆?/span>

鐩墠锛屽浗闄呬笂瀵逛簬纭崵鐜荤拑鏅跺寲鐨勭爺绌跺垰鍒氳捣姝ワ紝鍦ㄨ繖鏂归潰寮€灞曚簡杈冧负鍏ㄩ潰鐨勫伐浣滐紝浣嗙爺绌跺熀鏈笂灞€闄愪簬 [14-18]銆傛瘮濡傦紝 Lucas绛変汉閫氳繃鎺у埗缁勫垎涓庡姞鐑俯搴︼紝鍦?/span>GeSe2-Ga2Se3-CsCl涓潎鍖€鏋愬嚭Ga2Se3绾崇背鏅讹紝鍦ㄩ€忔槑鎬э紙杩戙€佷腑绾㈠娉㈡锛変笉鍙楀奖鍝嶇殑鍚屾椂锛屾湁鏁堝湴鎻愰珮浜嗘潗鏂欑殑鏈烘鎬ц兘锛屼娇鍏朵綔涓虹孩澶栫獥鍙f潗鏂欏叿鏈夐噸瑕佺殑搴旂敤鍓嶆櫙[17]銆備絾鏄紝鐢变簬Ga3+绂诲瓙鐨勫崐寰勬瘮绋€鍦熺瀛愬皬寰楀锛屼笉鍒╀簬鎺烘潅鐨勭█鍦熺瀛愪互缃崲鍥烘憾鐨勬柟寮忚繘鍏?/span>Ga2Se3鏅舵牸涓紝璇ユ潗鏂欏苟涓嶉€傚悎浣滀负绋€鍦熷彂鍏夊熀浣撱€傛渶杩戯紝鍥藉唴涓€浜涘崟浣嶅姝︽眽鐞嗗伐澶у銆佷笂娴风閰哥洂鐮旂┒鎵€銆佷笂娴锋妧鏈墿鐞嗙爺绌舵墍銆佸畞娉㈠ぇ瀛︺€佸崕涓滅悊宸ュぇ瀛︾瓑涔熷紑灞曚簡鏃ㄥ湪鏀硅繘纭崵鐜荤拑鏉愭枡鏈烘鎬ц兘鐨勬櫠鍖栫爺绌讹紝骞跺彇寰椾笉閿欑殑杩涘睍銆傞渶瑕佹寚鍑虹殑鏄紝杩勪粖鍥藉唴澶栭€氳繃鐮旂┒绋€鍦熸幒鏉傜~鍗ょ幓鐠冪殑鍙帶鏅跺寲鏉ユ彁楂樺叾涓孩澶栧彂鍏夌壒鎬э紝灏ゅ叾鏄帰绱㈡櫠鍖栫粨鏋勪笌绋€鍦熶腑绾㈠鍙戝厜鎬ц兘闂村叧绯荤殑宸ヤ綔灏?/span>寰堝皯鎶ラ亾銆?/span>

杩戝勾鏉ワ紝鎴戜滑璇鹃缁勫湪绋€鍦熸幒鏉傞€忔槑姘熸哀鍖栫墿鐜荤拑闄剁摲绾崇背澶嶅悎鏉愭枡鐨勫埗澶囥€侀暓绯绘盁鍖栫墿鏅跺寲涓庢樉寰粨鏋勮皟鎺с€佷互鍙婄█鍦熷厜璋辨€ц兘绛夋柟闈㈣繘琛屼簡澶ч噺鐨勭爺绌?/span>[13, 23-29]銆傜爺绌惰〃鏄庯紝鍏锋湁鑹ソ鍙戝厜鐗规€х殑绾崇背澶嶅悎鏉愭枡搴斿綋婊¤冻浠ヤ笅鍑犱釜鏉′欢锛氾紙1锛夊熀浣撴潗鏂欏湪娉垫郸鍏夎嚦鍙戝皠鍏夋尝娈佃寖鍥村叿鏈夎壇濂界殑閫忔槑鎬э紝鍥犺€屾潗鏂欎腑鐨勬櫠鍖栫浉搴斿崟鍒嗘暎鍧囧寑鍒嗗竷锛屼笖鏅剁矑灏哄害澶勪簬绾崇背閲忕骇锛涙垨鑰呮櫠鐩哥殑鎶樺皠鐜囦笌鐜荤拑鍩轰綋鐩歌繎锛屼互鍑忓皯鍏夋暎灏勶紱锛?/span>2锛変负浜嗛伩鍏嶆€ц兘鐨勭█閲婃晥搴旓紝鐗瑰畾鏅剁浉鐨勬櫠鍖栧垎鏁拌灏介噺楂橈紝鑰屽叾浠栨櫠鐩哥殑鏋愬嚭鍙楀埌瀹屽叏鎶戝埗锛涳紙3锛夌█鍦熺瀛愬懆鍥寸殑灞€鍩熸嫇鎵戠粨鏋勬湁搴忕▼搴﹂珮锛岀█鍦熸渶濂戒互缃崲鍥烘憾鐨勫舰寮忚繘鍏ョ撼绫虫櫠鏍硷紝浠ュ噺灏戝厜璋辩殑闈炲潎鍖€灞曞銆傝櫧鐒堕暓绯绘盁鍖栫墿鏅剁浉锛堝LaF3锛?/span>YF3锛?/span>NaYF4绛夛級瀵逛笁浠风█鍦熺瀛愬叿鏈夊緢楂樼殑鍥烘憾搴︼紝浣嗘盁姘у寲鐗╃幓鐠冮櫠鐡蜂綔涓虹█鍦熶腑绾㈠鍙戝皠鍩轰綋骞朵笉鍚堥€傦細棣栧厛锛屽浜庣█鍦熺殑涓孩澶栧彂灏勶紝姘熷寲鐗╁熀浣撶殑澹板瓙鑳介噺鍋忛珮锛涘叾娆★紝姘熸哀鍖栫墿鐜荤拑闄剁摲鐨勭孩澶栭€忚繃鎴娉㈤暱涓€鑸湪2.8um宸﹀彸锛屽洜鑰屽湪3-10um娉㈡鏄笉閫忔槑鐨勩€傚洜姝わ紝瑕佸彂灞曚紭鑹腑绾㈠鍙戝厜绾崇背澶嶅悎鏉愭枡锛屾湁蹇呰鐮旂┒鍚綆澹板瓙鑳介噺绾崇背鏅剁殑鏂板瀷鏉愭枡浣撶郴銆?/span>

鍩轰簬涓婅堪鑰冭檻锛屾垜浠棰樼粍鎻愬嚭閫氳繃鐔斾綋鎬ュ喎娉曞強鍚庣画鐑鐞嗗埗澶囩郴鍒楃█鍦熺瀛愭幒鏉傜殑銆侀暥宓?a name="OLE_LINK11">鐗瑰畾闀х郴姘寲鐗?/a>锛?a name="OLE_LINK2">濡?/a>LaCl3鎴?/span>YCl3绛夛級绾崇背鏅剁殑閫忔槑纭崵鍩虹撼绫冲鍚堟潗鏂欍€傜敱浜庝綔涓哄彂鍏変腑蹇冪殑绋€鍦熺瀛愪笌闀х郴姘寲鐗╃撼绫虫櫠鍖栫浉鐨勯槼绂诲瓙鍚屽睘闀х郴鍏冪礌锛屽洜姝よ緝瀹规槗閫氳繃鍥烘憾缃崲鐨勬柟寮忚繘鍏ユ櫠鏍间腑銆?a name="OLE_LINK30">閲嶇偣鐮旂┒闀х郴姘寲鐗╃殑鏅跺寲鍔ㄥ姏瀛﹀拰寰鏈虹悊銆佷互鍙婃隘鍖栫墿鐨勭粍鍒嗐€佺粨鏋勩€佸昂搴︺€佺粨鏅跺垎鏁板拰绋€鍦熸祿搴﹀鏉愭枡涓孩澶栧彂鍏夋€ц兘鐨勫奖鍝嶏紝浠ユ湡鑾峰緱鏈€浣虫垚鍒?/a>-缁撴瀯-鎬ц兘鐨勭粍鍚堬紝涓鸿繘涓€姝ュ紑鍙戞柊鍨嬩腑绾㈠婵€鍏夋潗鏂欐彁渚涘疄楠屼笌鐞嗚渚濇嵁銆?/span>

鐩墠鍒濇鐮旂┒缁撴灉琛ㄦ槑杩欑被鏉愭枡鏅跺寲鎺у埗鏄瘮杈冮毦鐨勶紝鏄撲簬鍑虹幇鏁翠綋鏋愭櫠鐨勬儏鍐碉紝鐩稿叧鐨勫伐浣滄垜浠棰樼粍姝e湪杩涜褰撲腑銆備笅鍥剧粰鍑鸿幏寰楃殑鍚?/span>Ga2S3绾崇背鏅剁殑纭崵鐜荤拑闄剁摲鐨勭數闀滅収鐗囥€?/span>

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鎾板啓璇ユ枃鐨勭洰鐨勬槸甯屾湜鏈夋洿澶氱殑鐮旂┒鑰呰兘澶熷紑灞曡繖鏂归潰鐨勫伐浣滐紝淇冭繘璇ョ被鏉愭枡鐨勭爺鍙戙€?/span>

锛堢増鏉冨綊浣滆€呮墍鏈夛紝璇峰嬁闅忎究鎷疯礉銆佽浆杞斤級

涓昏鍙傝€冩枃鐚?/span>

[1] S R Bowman, L B Shaw, B J Feldman, J Ganem, “A 7-µm praseodymium-based solid-state laser”, IEEE J. Quantum Electron., 32 (1996) 646–649

[2] 闄堢幃锛岀▼缁у缓锛岄檲鍥借崳锛?/span>鑻ュ共鏂板瀷闈炴哀鍖栫墿鐜荤拑鐨勭爺绌惰繘灞?/span>锛?strong style="mso-bidi-font-weight: normal">涓婃捣鍖栧伐锛?/span>24  (1999) 4-8

[3] Y S Xu, G Yang, W Wang, H D Zeng, X H Zhang, G R Chen, “Formation and properties of the novel GeSe2-In2Se3-CsI chalcohalide glasses”, J. Am. Ceram. Soc., 91 (2008) 902-905

[4] S Mao, H Z Tao, X J Zhao, G P Dong, “Microstructure and thermal properties of the GeS2-In2S3-CsI glassy system”, J. Non-Cryst. Solids., 354 (2008) 1298-1302

[5] G Tang, Z Y Yang, L Luo, W Chen, “Formation and properties of GeSe2-Ga2Se3-PbI2 novel chalcohalide glasses”, , 91 (2008) 1686-1689

[6] Z Y Yang, G Tang, L Luo, W Chen, “Visible transparent GeSe2-Ga2Se3-KX (X=I, Br or Cl) glasses for infrared optics”, J. Am. Ceram. Soc., 90 (2007) 667-669

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[8] V Moizan, V Nazabal, J Troles, P Houizot, J L Adam, J L Doualan, R Moncorg, F Smektala, G Gadret, S Pitois, G Canat, “Er3+ doped GeGaSbS glasses for mid-IR fiber laser application: synthesis and rare earth spectroscopy”,  Opt. Mater., 31 (2008) 39-46

[9] T H Lee, J Heo, “Energy transfer processes and Ho3+: 5I5 level population dynamics in chalcohalide glasses”, Phys. Rev. B 73 (2006) 144201

[10] 搴旂ゥ宀筹紝鑱傜鍗庯紝鎴翠笘鍕嬶紝寰愰搧宄帮紝閲戠弽濞燂紝澹板瓙妯″紡涓庣數瀛?/span>-澹板瓙缁撳悎寮哄害瀵?/span>Dy3+鎺烘潅纭掑寲鐗╃幓鐠冭崸鍏夋晥鐜囩殑褰卞搷锛?strong style="mso-bidi-font-weight: normal">鏃犳満鏉愭枡瀛︽姤锛?/span>23 (2008) 1125-1130

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[19] D H Zhao, X H Zhang, F Xia, H Wang, H L Ma, J L Adam, G R Chen, “Nonisothermal study on crystallization kinetics of GeSe2-As2Se3-CdSe chalcogenide glasses by differential scanning calorimeter”,  J. Cryst. Growth., 285 (2005) 228-235

[20] Z Y Yang, W Chen, H L Ma, X H Zhang, “Controlled crystallization of GeSe2-Ga2Se3-CsI chalcohalide glasses during molding”, J. Am. Ceram. Soc., 91 (2008) 2720-2723

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[28] D Q Chen, Y S Wang, Y L Yu, P Huang, F Y Weng, “Near-infrared quantum cutting in transparent nanostructured glass ceramics”, Opt. Lett., 33 (2008) 1884-1886

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